CTAB Assisted Synthesis of CuS Microcrystals： Synthesis, Mechanism, and Electrical Properties-中国期刊网

摘要 CuSmicrocrystalsweresuccessfullypreparedthroughamildsolvothermalreactioninethyleneglycol(EG)withtheassistanceofcationicsurfactantcetyltrimethylammoniumbromide(CTAB).Aninterestingmorphologyevolutionfromflower-likemicrospherestohollowmicrospheres,andfinallytosmoothnanoflakeswasobservedwhenincreasingtheamountofCTAB.TheproductswerecharacterizedbyX-raydiffraction(XRD),scanningelectronmicroscopy(SEM),transmissionelectronmicroscopy(TEM),andUV—visspectroscopy.ItwasfoundthattheamountofCTABplayedanimportantroleindeterminingthemorphologyoftheCuSmicrocrystals.Electricalmeasurementrevealsthattheas-preparedCuSmicrosphereswereofhighconductivity,whichmightfavortheirdeviceapplications.ItisexpectedthatCuSmicrocrystalswithcontrolledmorphologiesandstructureswillhaveimportantapplicationsinsolarcells.Thissimplebuteffectivemethodcouldalsobeextendedtothecontrolledgrowthofotherinorganicmicrocrystals.

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CTAB Assisted Synthesis of CuS Microcrystals： Synthesis, Mechanism, and Electrical Properties

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CTAB Assisted Synthesis of CuS Microcrystals： Synthesis, Mechanism, and Electrical Properties

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