简介:利用硬度分布函数计算8620H钢淬透性,以最优淬透性计算结果的各主要化学成分值为基础指导生产,采用化学成分窄范围设计,保证主要化学元素成分控制范围:w(C)为±0.0075%,w([Si])为±0.03%,w([Mn])、w([Cr])、w([Ni])为±0.02%,w([Mo])为±0.01%,w([Alt])为±0.010%,w([P])、w([S])不超过0.020%,w([B])不超过0.0005%,并控制碳偏析指数0.95~1.05。产品实测J(1.5)、J(5.0)、J(7.9)、J(12.7)淬透性满足要求,淬透性带宽达到不大于6HRC,甚至不大于4HRC的水平。
简介:Whitelight-emittingYVO_4:1mol.%Dy~(3+),xmol.%Eu~(3+)phosphorpowderswithordermorphologyandwellcrystallizationwerehydrothermallysynthesizedat180°C.Themicrostructure,white-lightemission,andlight-emittingmechanismofthepowderswerecarefullystudiedusingX-raydiffractometry,scanningelectronmicroscopyandphotoluminescencespectra.TheexcitationandemissionspectraofthephosphorpowdersindicatedthecoexistenceofefficientenergytransferfromEu~(3+)toDy~(3+)andinefficientenergytransferfromDy~(3+)toEu~(3+)besidestheenergytransferfromVO_4~(3–)toEu~(3+).IncreasingtheEu~(~(3+))concentrationinitiallyenhancedandthenweakenedtheluminescentintensityofDy~(3+).Thewhite-lightemissionsofYVO_4:1mol.%Dy~(3+),xmol.%Eu~(3+)phosphorpowderswerebothrelatedtotheenergytransferbetweenVO_4~(3–)andDy~(3+)/Eu~(3+),aswellasbetweenEu~(3+)andDy~(3+).TheinefficientenergytransferfromDy~(3+)toEu~(3+)wasfirstfound.
简介:文章采用电感耦合等离子原子发射光谱法测定滑石中MgO含量。将试样经硫酸、氢氟酸溶解,盐酸浸取,定容摇匀,用电感耦合等离子体原子发射光谱法直接测定,方法回收率在99.8%~100.3%之间,测定的RSD(n=6)在0.31%~1.86%之间。该方法简化了样品处理步骤,提高了工作效率,分析成本降低,适合批量样品分析。