简介：对304不锈钢2B板表面边鳞缺陷进行扫描电镜和能谱分析,并结合其整个生产工艺参数分析,得出铁素体当量高是导致边鳞缺陷发生的主要原因。根据上述原因提出了相应的改进建议。

简介：Themicrostructuresandprecipitatesinbasemetalsandheataffectedzones(HAZs)oftwoZr-Bmicroalloyedsteelswerecharacterizedbymeansofopticalmicroscopy(OM),transmissionelectronmicroscopy(TEM)andenergydispersivespectrum(EDS).Ithasbeenfoundthatprecipitatesoftensofnanometersinsizearepresentinthebasemetalsofbothsteels.Theaverageparticlesize,however,intheZr-BsteelwithTiislargerthanthatinthesteelwithoutTi.Afterthermalsimulations,inbothcases,theMnSsulfidescannucleateoncubic(Nb,Ti)(C,N)carbonitridesandnearlysphericalZr-bearingcompounds.TheprecipitatesintheHAZsofbothsteelsarecoarserthanthoseinthebasemetals,intherangesof150-200nmand50-100nmforTiaddedandTi-freesteels,respectively.

简介：采用碱熔处理样品，酸化后，移取部分溶液稀释后引入ICP测定ZrO2、TiO2、Fe2O3含量，剩余溶液用强碱分离钛、铁、锰等干扰元素后，EDTA—CuSO4法返滴定Al2O3，终点明显，检测重现性好；