简介:Thetungsten-inert-gas(TIG)arcweldingexperimentsofcementedcarbideYG30andsteel45werecarriedoutusingtheNi-Fe-Cfillingalloys.Theetaphasesandmechanicalpropertiesofweldedjointswereanalyzedbymeansofscanningelectronicmicroscope(SEM),transmissionelectronicmicroscope(TEM)coupledwithselecteddiffraction,electronicprobemicroanalysisandbendingstrengthmethods.Theexperimentalresultsshowthatthechemicalcompositionofthefillingalloysaffectsetaphaseformation.Whenthecarbonandnickelcontentsinfillingalloysare0.61wt%and55.29wt%,respectively,noetaphasesform.Andthejointbendingstrengthisthehighestto1.352GPa.Butiftheyare0.01wt%and55.38wt%,theetaphasesareformedattheboundariesofthecementedcarbideandtheweld,andthethicknessofetaphaselayerisabout110micrometers.Andthejointbendingstrengthislow.Usually,theseetaphasesareanomalouslygranular,andeasytoaccumulateattheboundariesbetweencementedcarbidesandtheweld.TheyaremultipleM6Crichintungstenandiron.
简介:摘要:探究化学分析过程中,经常会运用的两种技术就是化学分析及仪器分析。这两种技术在分析过程中,具有发挥精准、合理且科学的特点,对分析化学有着重要影响。本文就分析化学中的化学分析和仪器分析的原理、差异性、统一性及关联性进行解析,并提出二者今后的发展方向和趋势。 关键词:分析化学;化学分析;仪器分析