Carbonnanotube（CNTs）/Fe-Ni/TiO2nanocompositephotocatalystshavebeensynthesizedbyaninsitufluidizedbedchemicalvapordeposition（FBCVD）method.ThecompositephotocatalystswerecharacterizedbyXRD,Ramanspectroscopy,BET,FESEM,TEM,UV-visspectroscopy,andXPS.TheresultsshowedthattheCNTsweregrowninsituonthesurfaceofTiO2.Fe（lll）inTiO2showednochemicalchangesinthegrowthofCNTs.Ni（Ⅱ）waspartlyreducedtometalNiintheFBCVDprocess,andthemetalNiactedasacatalystforthegrowthofCNTs.ThephotocatalyticactivitiesofCNTs/Fe-Ni/TiO2decreasedwiththeriseoftheFBCVDreactiontemperature.ForthesamplesynthesizedatlowFBCVDtemperature（500℃）,morethan90%andnearly50%ofmethylenebluewereremovedunderUVirradiationin180minandundervisiblelightirradiationin300min,respectively.TheprobablemechanismofsynergisticenhancementofphotocatalysisontheCNTs/Fe-Ni/TiO2nanocompositeisproposed.
